Research Article | OPEN ACCESS
Effect of Temperature, pH and Concentration of Soluble Solids on the Rheological Behavior and Molecular Mass of Pectin Obtained from Mango Vallenato Shell (Mangifera indica l.)
1Ricardo Duran, 2Ramiro Torres and 2Yeimmy Peralta-Ruiz
1Universidad Popular del Cesar, Grupo Optimizaci
Advance Journal of Food Science and Technology 2018 SPL:35-40
Received: September 14, 2017 | Accepted: December 15, 2017 | Published: November 10, 2018
Abstract
The aim of the study was evaluating the incidence of pectin concentration, soluble solids concentration, extraction temperature and pH in the rheological behavior and molecular mass of a mango vallenato pectin gel. Experimental design was in blocks (mango pectin and commercial) completely random, in factorial arrangement 24, for the factors, pectin concentration (0.5-0.25% w/w), temperature (50, 70°C), pH (2.2- 2.8) and solids concentration (55, 65°Brix), with three replicates. Storage modulus (G’), loss modulus (G”) and loss tangent (tan δ), determined on the rheometer AR 1500 with parallel plate geometry, were determined. The data were adjusted to the Mark- Houwink-Sakurada model to determine the molecular weight of the pectin gel. Gels with 0.25% of mango pectin showed viscous behavior with little gelling property, the gels prepared with 50% of mango pectin at 55°Brix soluble solids concentration had a structured gel behavior, similar behavior to those of commercial pectin. The molecular mass of the gel prepared with mango pectin was in the range of 583.90 to 24.17 kDa, being significantly affected by the concentration of 0.25% of pectin, the extraction temperature and soluble solids concentration.
Keywords:
Complex viscosity, gel, loss modulus, loss tangent, storage modulus, thickener, viscoelasticity,
Competing interests
The authors have no competing interests.
Open Access Policy
This article is distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made.
Copyright
The authors have no competing interests.
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ISSN (Online): 2042-4876
ISSN (Print): 2042-4868 |
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