Research Article | OPEN ACCESS
Microwave-assisted Extraction and GC-MS Analysis of Zanthoxylum Oil from Zanthoxylum bungeanum
Xiaoguang Wang, Yueyun Yang and Ping Mi
College of Chemistry and Chemical Engineering, Zhoukou Normal University, Zhoukou Henan
466001, China
Advance Journal of Food Science and Technology 2015 9:723-726
Received: September 03, 2014 | Accepted: September 20, 2014 | Published: March 25, 2015
Abstract
The conditions for microwave-assisted extracting oil from Zanthorylum bungeanum seeds were studied and its chemical composition was analyzed by GC-MS. The effects of extract medium, microwave power, time and ratio of liquid to solid on extraction yield of Zanthorvlure bungeanum oil were investigated, using an orthogonal array design. The experimental results showed that using petroleum ether as extract medium, microwave power 350 w, solid-to-solvent ratio 1:5 (g/mL), 60 sec, can obtained 7.85% of Zanthorylum bungeanum oil. Thirty-three substances in Zanthorylum bungeanum oil were authenticated by GC-MS, of which 33 were identified for the first time and its chemical composition was analyzed. Accounting for 97.82% of the total volatile compounds.
Keywords:
Analyses, Gas Chromatography-Mass Spectrometry (GC-MS), microwave-assisted extraction, Zanthorylum bungeanum oil,
References
-
Borges, P., N. Fernandez and E. Roncal, 2004. Obtaining and characterizing of spices oleoresins. Alimentaria, 357: 97-99.
-
Bülow, N. and W.A. Konig, 2000. The role of Germacrene D as a precursor in sesquiterpene biosynthesis: Investigations of acid catalyzed, photochemically and thermally induced rearrangements. Phytochemistry, 2(55): 141-168.
CrossRef -
Fu, J., J. Gu and S. Fan, 2006. Studies on nutritional quality of asparagus spears of different varieties. J. Beijing Agric. Coll., 21(3): 26-28.
-
Gomes-Carneiro, M.R., I. Felzenszwalb and F.J. Paumgartten, 1998. Mutagenicity testing (+/-)-camphor, 1,8-cineole, citral, citronellal, (-)-menthol and terpineol with the salmonella/microsome assay. Mutat. Res., 1-2(416): 129-136.
CrossRef -
Magnusson, B.M., P. Runn, K. Karlsson and L.O.D. Koskinen, 1997. Terpenes and ethanol enhance the transdermal permeation of the tripeptide thyrotropin releasing hormone in human epidermis. Int. J. Pharm., 1(157): 113-121.
CrossRef -
Thomas, O.L., 1998. Volatile flavour production by Penicillium caseifulvum. Int. Dairy J., 8: 883-887.
CrossRef -
Wang, X., Y. Yang, P. Mi and R. Gang, 2014. Ultrasound-assisted extraction and GC-MS analysis of zanthoxylum oil from zanthoxylum. J. Chem. Pharmaceut. Res., 6(6): 2708-2712.
-
Zhao, Z.F., M. Lei, S.R. Lei, H.X. Quyang and Z. Yang, 2004. Experiment study on the extraction of xanthoxylin in different solvent. China Food Addit., 4: 18-21.
-
Zhou, X., G.Y. Liang, D.P. Wang and B.X. Xu, 2002. Study on the chemical constituents of the volatile oil from Lysimachia trientaloides Hemsl. Chin. J. Chromatogr., 20(3): 286-288.
-
Zhou, Z., X.P. Wang, J. Zhang and C. Cheng, 2001. Study on the application of microwave in extracting-tea polyphenols techniques. J. Hubei Inst. Natl. Nat. Sci., 19(32): 8-10.
Competing interests
The authors have no competing interests.
Open Access Policy
This article is distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made.
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The authors have no competing interests.
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